Synopsis ~ Labdanum and Cistus are not the same, but they come from the same plant and both have important use in perfumery – both with a luscious fragrant rich scent. This profile provides a detailed description with growth, description, chemistry, odor and uses.
LABDANUM/Cistus Resin & EO/Hydrosol Profile
By Jeanne Rose ~ July 2018
Cistus ladanifer – the plant that produces Cistus oil and Labdanum resin
INTRODUCTION: Labdanum and Cistus. This plain plant with its wondrous resin has been one of my favorites since I first learned of it back in 1969. I knew of Cistus as a plant growing in the San Francisco Arboretum but here in San Francisco it has very little odor as it doesn’t get hot enough. One day, some time ago, in June when it was clear, sunny and very hot I rubbed the leaves and they were sticky and fragrant. That is when I began to study it in my antiquarian herbals, one of which I had acquired back in 1970 (Dioscorides). How can anyone ignore a plant that was once harvested from the wool of goats?
COMMON NAME/LATIN BINOMIAL: CISTUS and LABDANUM are two products of the Cistus ladanifer (syn. ladaniferous) plant. Cistus is the essential oil distilled from the leaves and twigs of the same plant that produces the resin called Labdanum that is scraped from the leaves. Other Cistus species that are also used for Cistus EO and Labdanum resin include Cistus creticus and the subspecies incanus).
Family: Cistaceae is a family of perennial shrubs, flowering plants, found on dry and rocky soil with about 20 species.
Other Common Name/Naming Information: Cistus is from the Greek and simply means Rock rose because they frequent rocky-places, and this is a common name that is given to several other species of plants as well. The common Greek name is simply ladan. Cistus ladanifer is also called the gum Rockrose and the resin also called Ladanum.
Naming misinformation: Some people misspell and misuse the word Laudanum for Labdanum. Laudanum (a ‘u’ not a ‘b’) is a tincture of opium containing approximately 10% powdered opium by weight (the equivalent of 1% morphine). Reddish-brown and extremely bitter. Labdanum (with a ‘b’ not a ‘u’) is the resin from the plant Cistus.
COUNTRIES OF ORIGINS: Portugal, Morocco, Spain and the Canary Islands.
Eden Botanicals Harvest Location: Spain and my Cistus hydrosol is from Portugal.
ENDANGERED OR NOT: On the list of threatened plants.
GENERAL DESCRIPTION OF PLANT HABITAT AND GROWTH: Cistus ladanifer is an evergreen shrub and grows quickly to a height of about 5 feet and 3+ feet wide. They are thermophilous plants, meaning heat-loving and which require open, sunny places. It likes dry granitic hills with sandy well-drained soil and can tolerate heat, drought and sea exposure. It flowers in June, and though the flowers have both male and female parts, it is self-incompatible as the pollen can germinate and obstruct the stigma. Some books suggest that it is self-fertile. The plant is bee-pollinated. The flowers are white or pink with a simple structure. Cistus species are used as food plants by the larvae of some butterfly species. The petals are papery and crumpled, most commonly pure white, with numerous bright yellow stamens in the center and there is also a form which has a dark purple or crimson blotch at the base of each petal. The leaves are elongated and covered with glandular trichomes that secrete a viscous gummy balsam that exudes when it is hot. Because of the content of pinene, the plant is quite flammable, possibly can self-ignite, and is responsible for some serious fires. Spain is a leading producer of Labdanum.
PORTION OF PLANT USED IN DISTILLATION, HOW DISTILLED, EXTRACTION METHODS AND YIELDS:
There are four Labdanum products of the Cistus plant + one Cistus steam-distillate from the leaves and twigs: the gum collected from the leaves and twigs during the hottest time of the year; the resinoid produced by treating the gum with hot alcohol and concentrating it; the EO collected from the steam-distillation of the crude gum; and the concrete and absolute of Labdanum which are extracted by volatile solvents.
Labdanum resin is obtained by collecting and boiling the twigs in the spring and early summer, skimming off the resin as it comes to the surface. “Labdanum Absolute is obtained by solvent extraction of the resin – and is very much different in scent and color and viscosity from steam distilled Cistus essential oil from the leaves. The changing climate conditions, such as chilly early springs with very high summer temperatures, is contributing to lower yields, has reduced chemical complexity and increased the costs for the growers/collectors. However, both Labdanum and Cistus extractions result in intense, powerful aromas, used in very low percentages.” Yield: 0.1% – 0.2%
For Cistus essential oil, direct steam distillation of the young twigs and leaves produces the traditional quality essential oil of Spanish Cistus. The distillation yield is very low, only around 0.1% of the fresh plant.
Yield: Results are discussed from 0.1% to 0.3%.
ORGANOLEPTIC CHARACTERISTICS:
Odor Description/ Aroma Assessment:
Cistus EO has a peculiar, warm, fruity-floral scent, herbaceous and notes of moss, camphor, powder and leather-hay odor that is intense but less tenacious than Labdanum and is used with Lavender in spicy men’s products.
_____Labdanum has a rich, tenacious, but not intense odor of sweetness, smoky-woody, leather, powder, earthy-moss, with back notes of honey-animalic, floral with fruity overtones. It is an odor loved by me, by many and extraordinarily useful in many types of perfume application. It recalls the odor of ambergris and is in fact used as a vegetable substitute for ambergris in a perfume base note or as a fixative. The odor is tenacious in a blend but not intense, it lends a subtle richness to any perfume you use it in.
GENERAL PROPERTIES
Labdanum was historically known and used in herbal medicine for 1000s of years and is still used in the preparation of perfume. Cistus is considered antiviral, antibacterial, and anti-arthritic.
Cistus essential oil distilled from the leaves and twigs is considered a wound healer and as with most essential oils it has antiviral and antibacterial properties. Inhale the oil for a possible boost to the immune system and to reduce colds and infections resulting from the flu.
Cistus EO in the Arctander book
Labdanum is the sticky brown resin obtained from the shrubs Cistus ladanifer (western Mediterranean) and Cistus creticus (eastern Mediterranean), species of rockrose. It has a long history of use in herbal medicine and as a perfume ingredient.
Properties and Uses:
Cistus leaf tea is useful for children illness such as whooping cough and for adults for general all-over body inflammation.
Cistus tea is used as a treatment for Lyme Disease. The conclusion of the study, showed that to date, clinical work with wild harvested pure Sardinian Cistus tea and whole leaf Stevia is the least invasive yet most effective treatment for Lyme disease and many other modern chronic illnesses, caused by persistent and hidden infections. For more information read “Dr. Klinghardt Biological Lyme Protocol” at the Klinghardt Institute page. See the entire article at https://kiscience.com/sardinian-cistus-incanus/
Application/Skincare Uses: Cistus EO and tea has great application in skin care, particularly oily skin, acne skin and irritated skin. Use it in your lotions, other creams and clay masks using white clay. It is used for mature skin, wrinkles and the EO as an inhalant for coughs and bronchitis.
Cistus Anti-Wrinkle Lotion, a recipe by Jeanne Rose
I like to purchase an 8-oz bottle of pre-made unscented lotion with organically grown ingredients and then add my own special additions. If the lotion is thick I will thin it with some Rosemary or Cistus hydrosol until it is the texture that I like. Then I add 5 drops of Cistus EO to an ounce of my thinned lotion. I add the drops and with a long narrow thin wooden spoon, I stir in the EO, stirring around and around, up and down, figure 8 round and round. This is a sing-song that I do until the EO and hydrosol is thoroughly incorporated into the lotion. I only make an ounce at a time as it is easy to do and keeps the balance of the lotion fresh to make something else with. I apply this Cistus Lotion alternately with the Elemi/Galbanum Lotion every evening before bed.
https://jeanne-blog.com/elemi-resin-herb-eo/
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Emotional/Energetic Uses (AP or IN): Labdanum is used by inhalation and is considered to have a powerful ability to bring up past lives and past or buried memories. It is very helpful in ritual work.
Diffuse/Diffusion: Do not diffuse Labdanum as it is a sticky resin and even the steam-distilled product has the ability to gum up your diffusor. I suggest that you learn to use this substance in other ways and use the Labdanum and the Cistus essential oil in your perfumes.
HYDROSOL USES ~ Cistus hydrosol is available and just a wonderful product to use. It is bright and fresh and cleansing to the skin. I get mine from “Naturalness” in Portugal and it is available through them. This wonderful product is harvested using the stems and the leaves in the early morning until noon using pure gravity supplied water from a stream and steam-distillation. Use it as a spray after putting on make-up to set it, or on your clothes that have been crushed in a suitcase to freshen them or on the pillows before sleep. You can also carry it in your purse to spray on utensils before you use them and on hair or hands to refresh them. I am particularly fond of Cistus hydrosol.
The distiller recommends it : Cistus hydrosol is a powerful but gentle astringent. It is used as a daily toner for extremely oily, acne-prone, or irritated skin. For dry skin, only use as a 20% solution with other hydrosols or distilled water.
PLEASE NOTE: A true hydrosol should be specifically distilled for the hydrosol, not as a co-product or even a by-product of essential oil distillation. The plant’s cellular water has many components most are lost under pressurized short steam runs for essential oil, or by using dried material. We recommend that the producers specifically distill for a product by using plant material that is fresh.
HERBAL USES ~ “The use of the Cistus incanus has a long history and can be traced back to the 4th century BC. In the Middle East, northern Africa and the European Mediterranean region the Cistus incanus was enjoyed as a wellness tea for breakfast and indeed right throughout the day as a drink for relaxing after a strenuous day. When guests arrived, it was common to offer a freshly boiled pot of the Cistus tea. “The knowledge of the benefits of this tea were passed on late into the middle Ages.”3
See above for reference to the use of Cistus leaf tea as a treatment for Lyme disease.
JEANNE ROSE’S TOMATO TALES
A Personal Story of Labdanum
Labdanum resin/resinoid/absolute/EO is a favorite of mine and when I teach Perfumery classes I encourage the students to use my absolute that dates back to 1969. We make an old perfume called Chypre in the class. See formulas at the end and read my Natural Perfumery booklet.
Years ago, about 1970, I made a mixture of Labdanum resin that I had read in an old herbal that also used Benzoin and Storax with Civet, spike Lavender and spices. It was to be inhaled to ‘comforte the brain’. It looked interesting and certainly doable and whose brain does not need a certain amount of comforting. I found it was like playing with mud and very messy. I wrote about this in my first book, Herbs & Things, and if you want to try it, there are two recipes on pages 153-154.
These raw resins can stick almost permanently to everything. If you make it … “keep one mortar and pestle aside just for this type of recipe or for any recipe that calls for the heating of ‘beating’ of a resin. It was nearly impossible to roll the combination into a ball especially with the stinky civet, so I finally dipped my hands into the powdered Benzoin and Storax (sort of like dipping your hands into flour to roll out bread or cookie dough) and rolled the resin around. This gooey mess stuck very tenaciously to my hands and it took two days to wash it all off, but at least now I had a ball of resin. I then pierced the ball with a bodkin (big blunt needle with big eye) and hung it from a string.
It immediately oozed away from the string, plopped to the ground, and proceeded to ooze amoebically about the floor, peeling up paint as it went. It was then that I finally realized the exact nature of this pomander. It was and is ever-flowing and takes on the shape of whatever object it is on or in. I captured the now pancake-shaped resin, rolled more Storax into it and put in on the ledge above a window. Within a day it had migrated off the shelf and down the wall. It smelled deliciously but it left a trail of black resin (rather like the slime trail of a snail). Again, I captured it and this time rolled it up and stuck it in the freezer, to freeze. After thinking about it for some time I let it out of the freezer and put it immediately into a small black leather bag. We call it the Mental-Health Bag. The more you massage the bag, the more it smells, the better you feel, and the more powerful and tranquilizing its effect on the brain.”1 — Herbs & Things.
And I still have this fragrant Bag of Mental Health creeping around after 47 years.
Chemical Components: Comparison of Main Components: “The main components were α‐pinene (39%), viridiflorol (11.8%), ledol (3.3%) and bornyl acetate (3.1%). The occurrence of cyclosativene, γ‐cadinene, (E)‐β‐farnesene and β‐eudesmol in the essential oil of Cistus ladaniferus is reported here for the first time. Then, in order to study the chemical variability of individual oils, 20 samples were examined. α‐Pinene (11.1–47.4%) was the most abundant component in 18 of the 20 samples, followed by trans‐pinocarveol (4.4–10.9%) and viridiflorol (4.7–10.7%). Two samples exhibited a different chemical composition, not as yet described, characterized by the predominance of viridiflorol (20–22.6%), ledol (6.4–6.7%) and trans‐pinocarveol (5.4–8.6%).” © 1997 John Wiley & Sons, Ltd. — Composition of the Essential Oil of Cistus ladaniferus L. Cultivated in Corsica (France) by J. P. Mariotti , F. Tomi , J. Casanova , J. Costa , A. F. Bernardini , First published: 28 April 1999
Jeanne Rose collection of Cistus & Labdanum from 1972 to the present
HISTORY ~ The plant has been known since ancient times and has been described by Dioscorides, Herodotus and Pliny. Dioscorides says, “Now, that which we call Ladanum, is made of this plant. For the Hee goats, & shee goates, feeding on the leaues hereof, doe manifestly beare away the fatnesse of them on their beards and on their thighs, because it is of a viscous nature, which taken off thence they straine, & hauing fashioned them into little balls, lay them vp in store.”4
In ancient times, labdanum gum from Cistus creticus, a close relative of the species Cistus ladanifer – the only one used today – was collected in Crete in two ways: “Pliny says that the gum was harvested by combing the coats of goats that grazed in the cistus-covered hillsides; and later it was collected by thrashing the branches of the cistus plants with a leather strap and then scraping that strap with a knife. Cistus’ glutinous properties made these forms of harvesting possible. Today, most cistus production takes place in Spain, where the leafy branches are collected using a sickle before being processed.”2 But this may be where its history of being ‘leather scented’ comes from.
“In ancient Egypt, the false goat-hair beards of the pharaohs were impregnated with labdanum to surround these men with an impressive aura of distinction. The Cypriotes mixed Labdanum with Styrax and Calamus oil, thereby creating an early masterpiece of perfumery. The Crusaders, when they conquered the island, became so enthusiastic about the fragrance that they brought the recipe to the rest of Europe. It was known as the ‘Chypre’-theme, it is still employed in modern perfumery.”
Cistus creticus, has a subspecies, C. incanus , and is thought to be the ‘myrrh’ of Genesis. The resin of both are obtained by boiling twigs and skimming the resin from the surface of the water. —Mabberly.
NATURAL PERFUMERY
Labdanum is a sticky brown resin obtained from the shrubs Cistus ladanifer (western Mediterranean) and Cistus creticus (eastern Mediterranean), species of rockrose. It has a long history of use in herbal medicine and as a perfume ingredient. Labdanum is a powerful fixative in perfumery and is valued as a substitute to replace ambergris.
Modern uses –Labdanum is produced today mainly for the perfume industry. The raw resin is usually extracted by boiling the leaves and twigs. An absolute is also obtained by solvent extraction. An essential oil is produced by steam distillation.
The raw gum is a dark brown, fragrant mass containing up to 20% or more of water. It is plastic but not pourable and becomes brittle with age. The absolute is dark amber-green and very thick at room temperature. The fragrance more refined than the raw resin. The odor is very rich, complex and tenacious. Labdanum is much valued in perfumery because of its resemblance to ambergris.
In order to distinguish between Labdanum Absolute (which is usually the absolute from concrete extract of the plant material) and Labdanum Gum Absolute, the suppliers have resorted to using various odd names for their products. These products should have at least one thing in common: alcohol solubility. Labdanum Resin Absolute is a fairly logical designation for the alcoholic extract of crude Labdanum gum. In other words, it is an alcohol resinoid of Labdanum, prepared in a one-step hot or cold extraction. This product is also the cheapest of all the available alcohol soluble and generally applicable Labdanum extracts. Blends well with citrus oils.
To use the thick gum or the absolute in perfumery, it is most useful to dilute it 50•50 by volume with 95% neutral spirits (I prefer 95% neutral grape spirits). It will slowly dissolve in the alcohol, especially if kept warm or over a warm water bath. Always watch what you are doing and do not leave or abandon any warming resin in alcohol — that will surely be the time that something negative will happen.
Blends Best with: Labdanum – abs … The concrete is alcohol extracted to obtain the absolute. It is semi-solid soft and sticky green colored substance. It needs to be diluted in (grape spirits) alcohol to be used. The scent is balsam, herbal and spicy resin, warm and rich. Works well with citrus, Lavender bases, green and conifer scents. There are many types of absolute: from concrete, from resinoids. Labdanum 50•50 is Labdanum diluted 50% with neutral spirits. Various types of essential oil are produced by the steam-distillation of the leaves, twig and are usually called Cistus EO.
BLENDING
Galbanum & Labdanum/Cistus Base Accord
- Dilute each of your Galbanum and Labdanum 50•50 with neutral grape spirits.
- Let the above age and meld for a week.
- Take 12 drops of Galbanum (50•50) and 12 drops of (50•50) Labdanum (and Cistus if you wish) and mix together. Age it for 1-week. Smell and experience.
- After it ages, you can add equal amount of grape spirits to make a 25% pure scent base. Give it a name that you will remember.
A CHYPRE PERFUME
A Simple Chypre Perfume is made as follows:
5 drops of Bergamot + 5 drops White Grapefruit + 5 drops of Clary Sage with sclareol
1 drop of Oakmoss dissolved in several drops of alcohol
5 drops of Patchouli + 2 drops of Rose + 1 drop of Neroli
3 drops of Labdanum (pre-dilute in alcohol or purchase the Eden Botanicals Clear + 3 drops Atlas Cedarwood
The total equals 30 drops. Age this for at least 2 weeks (maybe more) and then add 90 drops of alcohol (95%) and age again for 3 weeks before you decide to do or not do anything else.
Equals 4 ml of finished scent at 25% perfume ingredients by volume.
INTERESTING INFORMATION: The Ladanesterion or lambadistrion is the tool made of leather leads used to comb out the Labdanum from the Cistus plant. It was described Pedanios Dioscorides in the 1st century AC. It was also described by the French botanist, Joseph Pitton de Tournefort, in his travel in Crete in 1700. The tool today has been replaced with plastic.
Abstract/Scientific Data: Anti-Dengue Virus Activity of the Oleoresin Labdanum of Cistus creticus.
During the epidemics of the mediaeval period, doctors in Byzantium and Italy developed the “Alipta muscata” as a preventive medicine against epidemics. When treating the “black death” doctors constantly used it for self-medication. The main ingredient of “Alipta muscata” was the oleoresin labdanum of Cistus creticus L. [1]. While the “black death” is mostly interpreted as Yersinia pestis, there is also an alternative interpretation as a viral hemorrhagic fever [2]. We tested several extracts and fractions of labdanum on their activity against the dengue virus (DENV-2 strain 00st-22A) in in vitro cultures on Vero cells (96-well-plates, 5 days). This haemorrhagic fever affects up to 500 million patients annually with no chemotherapeutic agent available and causes 20.000 deaths. Preliminary experiments with a labdanum full extract did not yield measurable results due to cytotoxic effects against Vero cells. In all following experiments, cell viability was constantly checked using the MTT-test. Fractionation of the dichloromethane raw-extract by liquid-liquid-extraction and column-chromatography on silica-gel (gradient elution with Hexane, EtOAc, CHCl3, MeOH) succeeded in separating the anti-viral activity of labdanum from its cytotoxic effect. In the most active fraction GS5 at 30 µg/ml, the dengue virus proliferation was 100% suppressed and cell viability over 90%. Structural elucidation of major constituents of GS5 is currently ongoing. Claims concerning the antiviral activity of above ground parts of C. creticus have been made previously, but these generally ascribe this activity to hot water soluble polyphenols and propose an unspecific tanning effect of the viral surface proteins as the mechanism of action [3]. We describe an antiviral activity of a dichloromethane extract of labdanum against a virulent hemorrhagic fever like dengue for the first time.
— https://www.thieme-connect.com/products/ejournals/abstract/10.1055/s-0037-1608551
KEY USE: The Oil of Perfumery
REFERENCES:
1Rose, Jeanne. Herbs & Things. Only available from jeannerose.net with coil binding.
2http://www.albertvieille.com/en/products/86-labdanum-resinoid-spain.html
3http://labdanum-creta.blogspot.com/2010/04/cistus-incanus-power-of-rock-rose-menu.html
4 Greek Herbal of Dioscorides. Hafner Publishing Company. 1933 from the great work of first century A.D.
Arctander, Steffen. Perfume and Flavor Materials of Natural Origin. Elizabeth, NJ. 1960
Guenther, Ernest. The Essential Oils. Volume VI. Reprint 1972.
Herbal Studies Course/ Jeanne Rose .2015 edition. San Francisco, California
http://www.andalucia.com/environment/wildflowers/the-gum-cistu
Langenheim, Jean H. Plant Resins. Timber Press. 2003
Mabberley, D. J. Mabberley’s Plant-Book, 3rd edition, 2014 printing, Cambridge University Press.
Pliny. Plinie’s Natural History. My copy is dated 1601.
Poucher, William A. Perfumes and Cosmetics. Van Nostrand Company. 1923
Rose, Jeanne. 375 Essential Oils and Hydrosols. Berkeley, California: Frog, Ltd., 1999
Rose, Jeanne. The Aromatherapy Book: Applications & Inhalations. North Atlantic Books. 2000
Rose, Jeanne. Natural Botanical Perfumery. JeanneRose.com. 2002
Sustainability: These items may not be sustainable in the amounts that are being used.
Endangered or not: Some of these plants are considered to be threatened and/or endangered due to heavy usage, people moving into the areas where they live and by over-tapping.
Do not Ingest essential oils: Although some oils are important flavoring oils in the flavor industry and thus ingested in very small amounts in many foods, especially meats and sausages, it is not a good idea to use them yourself either in capsules or honey to take internally.
Safety Precautions: Do not apply the essential oil neat, especially to the underarms or delicate parts of the body. Most resinous oils are probably not to be used on babies, children or pregnant women. Many aromatherapists suggest that there are some oils not be used at all. However, as with many plants, essential oil chemistry is subject to change depending on species and terroir.
Irritants: Some of the gums and resins can be quite irritating or sensitizing. Use the Patch Test before applying.
Patch Test: If applying a new essential oil to your skin always perform a patch test to the inner arm (after you have diluted the EO in a vegetable carrier oil). —Wash an area of your forearm about the size of a quarter and dry carefully. Apply a diluted drop (1 drop EO + 1 drop carrier) to the area. Then apply a loose Band-Aid and wait 24 hours. If there is no reaction, then go ahead and use the oil in your formulas. —The Aromatherapy Book, Applications & Inhalations, p. 64
DISCLAIMER: This work is intended for informational purposes only and is not a substitute for accurate diagnosis and treatment by a qualified health care professional. Dosages are often not given, as that is a matter between you and your health care provider. The author is neither a chemist nor a medical doctor. The content herein is the product of research and personal and practical experience. Institute of Aromatic & Herbal Studies – Jeanne Rose©
Labdanum Limerick
Labdanum is a resin that oozes
Diluted it works on your bruises
Cistus the leaf
Is good on beef
And in perfumery it always amuses.
—JeanneRose2018
Odor Profile of Labdanum resinoid diluted 50•50 with 95% grape alcohol
Amber Rosary beads with handmade linen thread – personalized
Amber bracelets, Amber oil, Amber succinite from China
Elemi EO and resin 2016 and 2018
Elemi oleo-Resin – 2018
5/27/18 At 9:30 A.M.
Elemi, the resin smells citrus